نوع مقاله : مقاله پژوهشی کامل
نویسندگان
1 گروه شیمی، دانشکده علوم پایه، دانشگاه پیام نور، تهران، ایران
2 واحد تحقیقات بالینی ، دانشکده پزشکی ، دانشگاه علوم پزشکی مشهد ، مشهد ، ایران
چکیده
چکیده
در این مقاله، یک روش جدید سریع و حساس مبتنی بر نانوکامپوزیت α-لینولنیک اسید Fe3O4 @ روکش دار با سدیم دودسیل سولفات همراه با کروماتوگرافی مایع با عملکرد بالا -آشکارساز آرایه دیودی (HPLC-PDA) برای استخراج و تعیین ترامادول (TRA) در نمونه های آب ارایه شده است. نانوذرات α -لینولنیک اسید Fe3O4 @ توسط طیف سنجی مادون قرمز تبدیل فوریه (FT-IR) ، میکروسکوپ الکترونی روبشی (SEM) و پراش اشعه ایکس (XRD) مشخص یابی شد. عوامل اصلی موثر بر استخراج و واجذب بهینه سازی شدند. در شرایط مطلوب ، روش با موفقیت برای تعیین TRA در نمونه های محیطی اعمال شد و خطی بودن خوب در محدوده 0.1-500 نانوگرم بر میلی لیتر (𝑅2> 0.99) بدست آمد. حد تشخیص (LOD) و انحراف استاندارد نسبی (RSD) به ترتیب 0.074نانوگرم بر میلی لیتر و 2.89٪ بود. سرانجام، روش پیشنهادی برای استخراج و تعیین ترامادول در نمونه های آبی با درصد بازیابی نسبی از 94 تا 103.97٪ با موفقیت اعمال شد.
کلیدواژه‌ها
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