نوع مقاله : مقاله پژوهشی کامل
نویسندگان
1 گروه شیمی، دانشگاه پیام نور، صندوق پستی 3697-19395 تهران، ایران
2 مرکز تحقیقات دارویی، انستیتوی نوروفورموکولوژی، دانشگاه علوم پزشکی کرمان، کرمان، ایران
چکیده
در این تحیقق، نانو زئولیت‌های Na/Al (ZAN) سنتز و شناسایی شدند، سپس یک الکترود کربن اصلاح شده (CPE) شده با ZAN برای اندازه گیری استامینوفن ساخته شد. مطالعات الکتروشیمیایی با ولتامتری رفت و برگشت خطی ولتامتری پالس تفاضلی انجام شد. این الکترود اصلاح شده در حضور استامینوفن به دلیل خواص الکتروکاتالیستی، پیک اکسیداسیون خاصی را در ولتاژ 59/0ولت نشان می دهد. حد تشخیص این روش 8/5 میکرومولار، انحراف استاندارد نسبی برای 7 اندازه گیری تکراری 1/1درصد و محدوده خطی کالیبراسیون برای تعیین استامینوفن 10 تا 115 میکرومولار است.
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